HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromopyrazolo[1,5-a]pyrimidine-2-carboxylic acid → HCID 71748063, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromopyrazolo[1,5-a]pyrimidine-2-carboxylic acid | HCID 771938 | — |
| Reactant | HCID 86697866 | HCID 86697866 | — |
| Product | HCID 71748063 | HCID 71748063 | — |
Reaction Steps
The title compound was prepared in accordance with the general method of example 1 from 6-Bromo-pyrazolo[1,5-A]pyrimidine-2-carboxylic acid and 3,4,5,6,7,8-hexahydro-thiazolo[4,5-d]azepin-2-one. The reaction mixture was purified by HPLC chromatography and lyophilized. Yield: 40 mg (49% of theory). ESI-MS: m/z=394 (M+H)+; Rt(HPLC): 1.11 min. (Method J).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09029360B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-237e2c679c364f85a787620e14b811ce |
| Source note | uspto-grants-2015_05 |