2-Aminopyridine → HCID 21855845, compound

HRID 572140Notes

Reaction equation

[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][N:3]=1.CO[C:10](OC)([N:12]([CH3:14])[CH3:13])[CH3:11]>>[CH3:13][N:12]([CH3:14])[C:10](=[N:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][N:3]=1)[CH3:11]

Participants

Reactant 2

HCID 104392-Aminopyridine

HCID 878351,1-Dimethoxyethyl(dimethyl)amine

Product 1

HCID 21855845HCID 21855845, compound

Procedure

Compound 13 was obtained according to general procedure I with 2-aminopyridine in presence of dimethylacetamide-dimethylacetal instead of dimethylformamide-dimethyl-acetal, as an orange oil in a quantitative yield.

Sources & evidence

ORD record: ord-85a9bfde45a14f5989fc453b597e2924
Source dataset: uspto-grants-2015_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09029393B2

Reaction notes

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