HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 178434648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 178434647 | HCID 178434647 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 178434648 | HCID 178434648 | 20% |
Reaction Steps
the title compound (30 mg) was prepared from crude 2-(5-amino-3-methyl-1H-pyrazol-4-yl)-benzothiazole-6-sulfonyl chloride (128 mg, 0.39 mmol), 4-methylpiperazine (39 mg, 0.43 mmol) and triethylamine (0.1 mL). MS (m/z, ES+): 393.1 (M+1,100%). Yield=20%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434720B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-1658c9a3d88744aa8933145669fc456e |
| Source note | uspto-grants-2016_09 |