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HRID572559

反应详情

EQUATION

反应方程式

HRID 572559 的结构方程式

REACTANTS

反应物

2
结构：N#Cc1ccc(CBr)c(F)c1
HCID2783149

4-(Bromomethyl)-3-fluorobenzonitrile

C8H5BrFN

结构：CC(C)(C)OC(=O)C(C)(C)N
HCID7019940

tert-Butyl 2-methylalaninate

C8H17NO2

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)C(C)(C)NCc1ccc(C#N)cc1F
HCID66652709

未命名化合物

PROCEDURE

实验过程

The title compound was prepared following general procedure 10 starting from tert-butyl 2-amino-2-methylpropanoate and 4-cyano-2-fluoro benzyl bromide. The title compound was isolated as colorless liquid. 1H NMR (DMSO-d6, 400 MHz) δ 7.78-7.75 (d, J=10.0 Hz, 1H), 7.71-7.65 (m, 2H), 3.70-3.68 (d, J=6.9 Hz, 2H), 2.55 (s, 1H), 1.44 (s, 9H), 1.19 (s, 6H).

WORKUP

后处理

  1. customThe title compound was prepared