HCID 86719102, compound → HCID 86719101, compound

HRID 572919Notes

Reaction equation

HRID 572919 reaction equation
[N+:1]([C:4]1[C:5]([CH2:10][C:11]([O:13][CH3:14])=[O:12])=[N:6][CH:7]=[CH:8][CH:9]=1)([O-])=O>CO>[NH2:1][C:4]1[C:5]([CH2:10][C:11]([O:13][CH3:14])=[O:12])=[N:6][CH:7]=[CH:8][CH:9]=1

Participants

3

Reactant 1

HCID 86719102HCID 86719102, compound

Product 1

HCID 86719101HCID 86719101, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Methyl 2-(3-nitropyridin-2-yl)acetate (1 g, 5 mmol) was dissolved in MeOH and stirred under the atmosphere of H2 at room temperature overnight. LC-MS find the desired product. It was filtered through a pad of Celite and evaporated to get the desired product. It was directly used for the next step. LC-MS: m/z (M+H)=167.1

Sources & evidence

ORD record
ord-088aa8b9d8474320b98d833ee585ce72
Source dataset
uspto-grants-2015_05
Patent number
US09029531B2

Reaction notes

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