HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86719102, compound → HCID 86719101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86719102 | HCID 86719102 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86719101 | HCID 86719101 | — |
Reaction Steps
Methyl 2-(3-nitropyridin-2-yl)acetate (1 g, 5 mmol) was dissolved in MeOH and stirred under the atmosphere of H2 at room temperature overnight. LC-MS find the desired product. It was filtered through a pad of Celite and evaporated to get the desired product. It was directly used for the next step. LC-MS: m/z (M+H)=167.1
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09029531B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-088aa8b9d8474320b98d833ee585ce72 |
| Source note | uspto-grants-2015_05 |