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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 572938Generated: October 31, 2026

HCID 86719116, compound → HCID 86719117, compound

https://huagongshe.com/reaction/572938

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86719116HCID 86719116—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 86719117HCID 86719117—

Reaction Steps

The solution of tert-butyl 4-(3-(2-methoxy-2-oxoethyl)phenyl)-5,6-dihydropyridine-1(2H)-carboxylate (330 mg, 1.0 mmol) and Pd/C (30 mg) in methanol (10 mL) was stirred under H2 at room temperature for 12 h. Then, the reaction mixture was filtered and evaporated under reduced pressure to get desired product for the next step without further purification. LC-MS: m/z (M+H)=334.4

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09029531B2
Source datasetuspto-grants-2015_05
ORD IDord-f42de9b5443a4e2398b9ebad600f495c
Source noteuspto-grants-2015_05