HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86719116, compound → HCID 86719117, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86719116 | HCID 86719116 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86719117 | HCID 86719117 | — |
Reaction Steps
The solution of tert-butyl 4-(3-(2-methoxy-2-oxoethyl)phenyl)-5,6-dihydropyridine-1(2H)-carboxylate (330 mg, 1.0 mmol) and Pd/C (30 mg) in methanol (10 mL) was stirred under H2 at room temperature for 12 h. Then, the reaction mixture was filtered and evaporated under reduced pressure to get desired product for the next step without further purification. LC-MS: m/z (M+H)=334.4
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09029531B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-f42de9b5443a4e2398b9ebad600f495c |
| Source note | uspto-grants-2015_05 |