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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 573613Generated: October 29, 2026

Benzenesulfonyl chloride → HCID 68324140, compound

https://huagongshe.com/reaction/573613

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzenesulfonyl chlorideHCID 7369—
ReactantHCID 68324016HCID 68324016—
ProductHCID 68324140HCID 6832414019.1%

Reaction Steps

Following the general method as outlined in Example 28, starting from 2,6-dimethyl-3-phenylthieno[2,3-b]pyridin-4-amine (97 mg, 0.381 mmol) (Description 10) and benzenesulfonyl chloride (135 mg, 0.763 mmol), the title compound (28.7 mg) was isolated. LCMS (A) m/z: 395 [M+1]+, Rt 0.96 min (basic), Rt 1.39 min (acidic).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09029545B2
Source datasetuspto-grants-2015_05
ORD IDord-5188d18411cb4a59bd39d3b9c90f6e8e
Source noteuspto-grants-2015_05