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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 573627Generated: November 2, 2026

Trifluoroacetic acid → HCID 68380820, compound

https://huagongshe.com/reaction/573627

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
Reactant1-methyl-1H-imidazole-4-sulfonyl chlorideHCID 2736887—
ReactantHCID 68324020HCID 68324020—
ProductHCID 68380820HCID 68380820—

Reaction Steps

Following general method outlined in Example 1, starting from 3-[3,4-bis(methyloxy)phenyl]-6-methylthieno[2,3-b]pyridin-4-amine (62 mg, 0.150 mmol) (Description 24) and 1-methyl-1H-imidazole-4-sulfonyl chloride (54.0 mg, 0.299 mmol), the title compound (26 mg) was isolated as a TFA salt. LCMS (B) m/z: 445 [M+1]+, Rt 2.41 min.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09029545B2
Source datasetuspto-grants-2015_05
ORD IDord-d11807b429a24cbfa418b271a43ccaf5
Source noteuspto-grants-2015_05