HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 68380820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 1-methyl-1H-imidazole-4-sulfonyl chloride | HCID 2736887 | — |
| Reactant | HCID 68324020 | HCID 68324020 | — |
| Product | HCID 68380820 | HCID 68380820 | — |
Reaction Steps
Following general method outlined in Example 1, starting from 3-[3,4-bis(methyloxy)phenyl]-6-methylthieno[2,3-b]pyridin-4-amine (62 mg, 0.150 mmol) (Description 24) and 1-methyl-1H-imidazole-4-sulfonyl chloride (54.0 mg, 0.299 mmol), the title compound (26 mg) was isolated as a TFA salt. LCMS (B) m/z: 445 [M+1]+, Rt 2.41 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09029545B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-d11807b429a24cbfa418b271a43ccaf5 |
| Source note | uspto-grants-2015_05 |