Acetic Acid → HCID 86623302, compound

HRID 574048Notes

Reaction equation

HRID 574048 reaction equation
[CH3:1][O:2][SiH:3]([O:6][CH3:7])[O:4][CH3:5].C(O)(=O)C.[CH3:12][O:13][CH2:14][O:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH:24]=[CH2:25]>>[CH3:12][O:13][CH2:14][O:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][Si:3]([O:6][CH3:7])([O:4][CH3:5])[O:2][CH3:1]

Participants

4

Reactant 3

HCID 176Acetic AcidHCID 17215TrimethoxysilaneHCID 85607836HCID 85607836, compound

Product 1

HCID 86623302HCID 86623302, compound

Procedure

Under a nitrogen atmosphere at 80° C., a mixture of 64 g of trimethoxysilane and 0.57 g of acetic acid was dropped in a mixture of 100 g of 10-(methoxymethoxy)-1-decene and a catalytic amount of a solution of tetrahydrofuran chloroplatinate. The resultant mixture was stirred for 3 hours at 80° C., and then the reaction mixture was distilled under reduced pressure, to obtain 131 g of an intended substance.

Workup

  1. distillationthe reaction mixture was distilled under reduced pressure
  2. customto obtain 131 g of an intended substance

Sources & evidence

ORD record
ord-d3763fe665164f28bed87dc0196aa4d9
Source dataset
uspto-grants-2015_05
Patent number
US09034661B2

Reaction notes

Loading…