Acetic Acid → HCID 86623302, compound

Participants

Reaction Steps

Under a nitrogen atmosphere at 80° C., a mixture of 64 g of trimethoxysilane and 0.57 g of acetic acid was dropped in a mixture of 100 g of 10-(methoxymethoxy)-1-decene and a catalytic amount of a solution of tetrahydrofuran chloroplatinate. The resultant mixture was stirred for 3 hours at 80° C., and then the reaction mixture was distilled under reduced pressure, to obtain 131 g of an intended substance.

Provenance & Evidence