Hydrochloric Acid → HCID 66807131, compound

Participants

Reaction Steps

43 mg (68 μmol) of the compound of Example 7 were dissolved in 3 ml of methanol, and 273 μl of a 1M aqueous lithium hydroxide solution (0.27 mmol) were added. The mixture was stirred at RT overnight and then acidified by addition of 1N hydrochloric acid and diluted with water. The precipitated solid was filtered off with suction, washed with a little water and dried in a vacuum drying cabinet at 50° C. This gave 32 mg (74% of theory) of the title compound.

Provenance & Evidence