Hydrazine, (4-chlorophenyl)-, hydrochloride (1:1) → HCID 57875947, compound

HRID 574443Notes

Reaction equation

HRID 574443 reaction equation
Br[CH2:2][C:3]([N:5]1[CH2:10][CH2:9][CH2:8][CH2:7][C:6]1([CH3:12])[CH3:11])=[O:4].Cl.[Cl:14][C:15]1[CH:20]=[CH:19][C:18]([NH:21]N)=[CH:17][CH:16]=1.[CH3:23][N:24]1[CH2:29][CH2:28][C:27](=O)[CH2:26][CH2:25]1>C(N(CC)CC)C>[Cl:14][C:15]1[CH:20]=[CH:19][C:18]2[N:21]([CH2:2][C:3]([N:5]3[CH2:10][CH2:9][CH2:8][CH2:7][C:6]3([CH3:12])[CH3:11])=[O:4])[C:27]3[CH2:28][CH2:29][N:24]([CH3:23])[CH2:25][C:26]=3[C:17]=2[CH:16]=1

Participants

5

Reactant 3

HCID 71600Hydrazine, (4-chlorophenyl)-, hydrochloride (1:1)HCID 740491-Methyl-4-piperidoneHCID 68928255HCID 68928255, compound

Product 1

HCID 57875947HCID 57875947, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The title compound is prepared by following Method 8 by using 2-bromo-1-(2,2-dimethylpiperidin-1-yl)ethanone, 4-chlorophenylhydrazine hydrochloride, triethylamine and N-methyl-4-piperidone.

Sources & evidence

ORD record
ord-cadcaa7730ab45de86dd31e290863548
Source dataset
uspto-grants-2015_05
Patent number
US09034880B2

Reaction notes

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