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HRID574557

反应详情

EQUATION

反应方程式

HRID 574557 的结构方程式

REACTANTS

反应物

3
结构：[K+].[OH-]
HCID14797

Potassium hydroxide

HKO

结构：Cc1ccc2[nH]c3c(c2c1)CN(C)CC3
HCID209291

1H-Pyrido(4,3-b)indole, 2,3,4,5-tetrahydro-2,8-dimethyl-

C13H16N2

结构：C=Cc1ccc(OC)nc1
HCID23070135

5-Ethenyl-2-methoxypyridine

C8H9NO

PRODUCTS

生成物

1
结构：COc1ccc(CCn2c3c(c4cc(C)ccc42)CN(C)CC3)cn1
HCID57876385

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN1CCCC1=O
溶剂HCID13387

N-Methyl-2-pyrrolidone

C5H9NO

PROCEDURE

实验过程

The title compound is prepared from a mixture of 2,3,4,5-tetrahydro-2,8-dimethyl-1H-pyrido[4,3-b]indole, 2-methoxy-5-vinylpyridine and KOH (5-7 equiv) in NMP at a temperature ranging between 25 deg C. to 100 deg C. The product obtained is isolated by preparative HPLC.

WORKUP

后处理

  1. customranging between 25 deg C
  2. customto 100 deg C
  3. customThe product obtained
  4. customis isolated by preparative HPLC