HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-ethyl-2-isothiocyanato-5-methylthiophene-3-carboxylate → 2,3-dihydro-5,6-dimethyl-3-(3-(4-methyl-1H-imidazol-1-yl)propyl)-2-thioxothieno[2,3-d]pyrimidin-4(1H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-ethyl-2-isothiocyanato-5-methylthiophene-3-carboxylate | HCID 4513532 | — |
| Reactant | 3-(4-Methyl-1H-imidazol-1-yl)propan-1-amine | HCID 15034954 | — |
| Product | 2,3-dihydro-5,6-dimethyl-3-(3-(4-methyl-1H-imidazol-1-yl)propyl)-2-thioxothieno[2,3-d]pyrimidin-4(1H)-one | HCID 25100358 | — |
Reaction Steps
The compound was synthesized starting from methyl 4-ethyl-2-isothiocyanato-5-methylthiophene-3-carboxylate (0.110 g. 0.46 mmol) and 3-(4-methyl-1H-imidazol-1-yl)propan-1-amine (9) (0.063 g, 0.46 mmol) as described above.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09034907B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-7ff126a410d9488c96493da469c722b4 |
| Source note | uspto-grants-2015_05 |