HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58979602, compound → HCID 71715107, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58979602 | HCID 58979602 | — |
| Reactant | 10-Bromo-9-fluoro-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine-2-carboxamide | HCID 86693051 | — |
| Product | HCID 71715107 | HCID 71715107 | 40% |
Reaction Steps
Similar to as described in General Procedure G, 10-bromo-9-fluoro-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine-2-carboxamide was reacted with 1,1,1-trifluoro-2-methylbut-3-yn-2-ol (US2005/250741 A1) to give the titled compound as a white solid (80 mg, 40%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09034866B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-375f56ace5084da3a2087e4182f2710d |
| Source note | uspto-grants-2015_05 |