HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pentynenitrile, 3-hydroxy-3-methyl- → HCID 86693242, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pentynenitrile, 3-hydroxy-3-methyl- | HCID 12298493 | — |
| Reactant | 10-Bromo-9-fluoro-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine-2-carboxamide | HCID 86693051 | — |
| Product | HCID 86693242 | HCID 86693242 | 30% |
Reaction Steps
Similar to as described in General Procedure G, 10-bromo-9-fluoro-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine-2-carboxamide was reacted with 3-hydroxy-3-methylpent-4-ynenitrile to give the titled compound as a brown solid (70 mg, 30%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09034866B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-7319ad482c044730bf537b058c6cfd42 |
| Source note | uspto-grants-2015_05 |