huagongshe.com
HRID575305

反应详情

EQUATION

反应方程式

HRID 575305 的结构方程式

REACTANTS

反应物

2
结构：C#C[C@@](C)(O)c1cc(C)on1
HCID58221468

未命名化合物

结构：CNC(=O)c1c(C(N)=O)nn2c1CCOc1ccc(Br)cc1-2
HCID86693336

未命名化合物

PRODUCTS

生成物

1
结构：CNC(=O)c1c(C(N)=O)nn2c1CCOc1ccc(C#C[C@@](C)(O)c3cc(C)on3)cc1-2
HCID86693337

未命名化合物

收率 26%

PROCEDURE

实验过程

Similar to as described in General Procedure G, 9-bromo-N3-methyl-4,5-dihydrobenzo[b]pyrazolo[1,5-d][1,4]oxazepine-2,3-dicarboxamide was reacted with (R)-2-(5-methylisoxazol-3-yl)but-3-yn-2-ol to give the titled compound as an off-white solid (37 mg, 26%).