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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 575657Generated: October 29, 2026

Ethanesulfonamide → US10023592, Example 168

https://huagongshe.com/reaction/575657

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanesulfonamideHCID 73702—
ReactantUS10023592, Example 150HCID 118021426—
ProductUS10023592, Example 168HCID 118021498—

Reaction Steps

The title compound of Example 150 was treated with EtSO2NH2 instead of MeSO2NH2 in a manner similar to Example 152, step 6 to give the title compound. 1H NMR (CDCl3, 400 MHz) δ 8.35 (d, J=2.0 Hz, 1H), 8.18 (s, 1H), 7.70 (d, J=2.0 Hz, 1H), 7.25-7.22 (m, 1H), 7.12-7.07 (m, 1H), 7.04-7.01 (m, 1H), 3.93 (s, 3H), 3.70 (s, 3H), 3.38 (s, 3H). LCMS: 423.9 (M+1)+

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09034900B2
Source datasetuspto-grants-2015_05
ORD IDord-b1aeab643e3048ae979d4d73846ad2ed
Source noteuspto-grants-2015_05