HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-((Dibenzylamino)methyl)morpholin-3-one → 6-(Aminomethyl)morpholin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-((Dibenzylamino)methyl)morpholin-3-one | HCID 9995550 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 6-(Aminomethyl)morpholin-3-one | HCID 10057542 | — |
Reaction Steps
A solution of 6-((dibenzylamino)methyl)morpholin-3-one (340 mg, 1.09 mmol), Pd(OH)2/C (170 mg) in EtOH (30 mL) was stirred equipped under H2 balloon overnight. The solution was filtered and concentrated to give white oil. The crude product was used directly for next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434726B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-bbc83b480d1644d2811adaf60dc45bb8 |
| Source note | uspto-grants-2016_09 |