HRID57599

反应详情

EQUATION

反应方程式

HRID 57599 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 6-((dibenzylamino)methyl)morpholin-3-one (340 mg, 1.09 mmol), Pd(OH)2/C (170 mg) in EtOH (30 mL) was stirred equipped under H2 balloon overnight. The solution was filtered and concentrated to give white oil. The crude product was used directly for next step without purification.

WORKUP

后处理

  1. customequipped under H2 balloon overnight
  2. filtrationThe solution was filtered
  3. concentrationconcentrated
  4. customto give white oil
  5. customThe crude product was used directly for next step without purification