Tetrahydrofuran → HCID 89375853, compound

Participants

Reaction Steps

To a solution of 0.10 g like-8,8′-(oxirane-2,3-diyl)dioctanenitrile in 5.0 g THF was added 0.50 mL of a solution of 0.0988 g 70% HClO4 in 1.9104 g water. After standing for 24 h at room temperature, the mixture was diluted with 250 mL CH2Cl2, which resulted in the separation of aqueous droplets. The mixture was dried over Na2CO3 and evaporated to afford 0.10 g of product as a white powder.

Provenance & Evidence