HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → (9H-fluoren-9-yl)methyl hexahydropyrrolo[3,4-b]pyrrole-1 (2H)-carboxylate hydrochloric acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-(9H-fluoren-9-yl)methyl 5-tert-butyl hexahydropyrrolo[3,4-b]pyrrole-1,5-dicarboxylate | HCID 71113792 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (9H-fluoren-9-yl)methyl hexahydropyrrolo[3,4-b]pyrrole-1 (2H)-carboxylate hydrochloric acid | HCID 86717379 | — |
Reaction Steps
1-(9H-fluoren-9-yl)methyl 5-tert-butyl hexahydropyrrolo[3,4-b]pyrrole-1,5-dicarboxylate (810 mg, 1.86 mmol) was treated with HCl in MeOH (5 mL) for 2 hours and then concentrated in vacuo to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434726B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-4da18fe442634f1a8fa28fa1fc033ed0 |
| Source note | uspto-grants-2016_09 |