HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Dioxide → Caesium stearate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | Stearic Acid | HCID 5281 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | Caesium stearate | HCID 23720211 | — |
Reaction Steps
A mixture of Cs2CO3 and stearic acid was added to butanol in the ratio 1:2 and kept at reflux temperature until no more CO2 formed. Subsequently, butanol was separated on the rotary evaporator, the residue mixed with ether and aspirated, m.p.:263-269° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040112B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-89685cf973f9440c968721127bded328 |
| Source note | uspto-grants-2015_05 |