HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Bromomethyl)-1,3,4-trichlorobenzene → HCID 178516528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Bromomethyl)-1,3,4-trichlorobenzene | HCID 78662 | — |
| Reactant | 2-sulfanylpyrimidin-4-ol | HCID 178516529 | — |
| Product | HCID 178516528 | HCID 178516528 | 89% |
Reaction Steps
As per procedure from Example 1, this compound was prepared from 2-(bromomethyl)-1,3,4-trichlorobenzene and 2-sulfanylpyrimidin-4-ol to provide the title compound as a white solid (1.04 g, 89% yield); 1H NMR (400 MHz, DMSO-do): δ 4.72 (s, 2H), 6.21 (bs, 1H), 7.58 (d, J=8.8 Hz 1H), 7.68 (d, J=8.8 Hz 1H), 8.02 (bs, 1H); M+ 322.8.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040538B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-0a80ab69f682463ebbbdca7727bd99f0 |
| Source note | uspto-grants-2015_05 |