HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 21250395, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Benzoic acid, 4-amino-3-nitro- | HCID 74115 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21250395 | HCID 21250395 | — |
Reaction Steps
A mixture of 4-amino-3-nitro-benzoic acid (12.0 g, 65.9 mmol) in 300 mL dichloromethane with 12 mL thionyl chloride was refluxed for 2.5 h, and concentrated to dryness i. vac. The residue was further reacted without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040565B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-1837c779c25244279c70300c2e6ca2d7 |
| Source note | uspto-grants-2015_05 |