HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 695751, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3,4-Dichlorobenzoic acid | HCID 5817 | — |
| Reactant | N-Hydroxynicotinimidamide | HCID 308113 | — |
| Product | HCID 695751 | HCID 695751 | — |
Reaction Steps
The title compound was prepared according to the procedure of Example 8 using N′-hydroxynicotinimidamide (Aldrich) and 3,4-dichlorobenzoic acid (Aldrich). 1H NMR (300 MHz, CD3OD) δ 7.64 (ddd, J=8.0, 5.1, 0.8 Hz, 1H), 7.82 (d, J=8.3 Hz, 1H), 8.14-8.19 (m, 1H), 8.40 (d, J=2.0 Hz, 1H), 8.56 (dt, J=7.9, 2.0 Hz, 1H), 8.75 (dd, J=5.2, 1.6 Hz, 1H), 9.29 (dd, J=2.2, 1.0 Hz, 1H) ppm; MS (DCI/NH3) m/z 292 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040568B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-e558e50695f04788a76b0f7d94c19822 |
| Source note | uspto-grants-2015_05 |