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HRID578130

反应详情

EQUATION

反应方程式

HRID 578130 的结构方程式

REACTANTS

反应物

3
结构：N
HCID222

Ammonia gas

H3N

结构：CN
HCID6329

Methylamine

CH5N

结构：O=C(O)c1cccc(S(=O)(=O)Cl)c1
HCID77641

Benzoic acid, 3-(chlorosulfonyl)-

C7H5ClO4S

PRODUCTS

生成物

1
结构：CNS(=O)(=O)c1cccc(C(=O)O)c1
HCID252654

3-methylsulfamoyl-benzoic acid

C8H9NO4S

PROCEDURE

实验过程

The title compound was prepared according to the procedure of Example 50A using 3-(chlorosulfonyl)benzoic acid (Aldrich) and methylamine (Aldrich). 1H NMR (300 MHz, CD3OD) δ 2.54 (s, 3H), 7.70 (t, J=7.8 Hz, 1H), 8.02-8.07 (m, 1H), 8.23-8.28 (m, 1H), 8.45 (t, J=1.9 Hz, 1H) ppm; MS (DCI/NH3) m/z 233 (M+NH4)+.