Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → 3-(Methylsulfamoyl)benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | Methylamine | HCID 6329 | — |
| 반응물 | Benzoic acid, 3-(chlorosulfonyl)- | HCID 77641 | — |
| 생성물 | 3-(Methylsulfamoyl)benzoic acid | HCID 252654 | — |
반응 단계
The title compound was prepared according to the procedure of Example 50A using 3-(chlorosulfonyl)benzoic acid (Aldrich) and methylamine (Aldrich). 1H NMR (300 MHz, CD3OD) δ 2.54 (s, 3H), 7.70 (t, J=7.8 Hz, 1H), 8.02-8.07 (m, 1H), 8.23-8.28 (m, 1H), 8.45 (t, J=1.9 Hz, 1H) ppm; MS (DCI/NH3) m/z 233 (M+NH4)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09040568B2 |
| 출처 데이터셋 | uspto-grants-2015_05 |
| ORD ID | ord-923d78e90ce9427b8992c6633b2c2765 |
| 출처 메모 | uspto-grants-2015_05 |