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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 578183Generated: October 31, 2026

Ammonia → HCID 44545068, compound

https://huagongshe.com/reaction/578183

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantN-HydroxynicotinimidamideHCID 308113—
Reactant1H-Indazole-5-carboxylic acidHCID 4248454—
ProductHCID 44545068HCID 44545068—

Reaction Steps

The title compound was prepared according to Method C using 1H-indazole-5-carboxylic acid (ABCR) and N′-hydroxynicotinimidamide (Tyger). 1H NMR (300 MHz, DMSO-d6) δ 7.7 (dd, J=7.9, 4.8 Hz, 1H), 7.8 (d, J=8.7 Hz, 1H), 8.2 (dd, J=8.7, 1.6 Hz, 1H), 8.4 (s, 1H) 8.5 (dt, J=7.9, 1.8 Hz, 1H), 8.7 (s, 1H) 8.8 (dd, J=4.8, 1.6 Hz, 1H), 9.3 (d, J=2.0 Hz, 1H), 13.6 (s, 1H) ppm; MS (DCI/NH3) m/z 264 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09040568B2
Source datasetuspto-grants-2015_05
ORD IDord-7fcda079d2ea4615b6694fb8982b2a9b
Source noteuspto-grants-2015_05