HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 53482764, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 53482763 | HCID 53482763 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53482764 | HCID 53482764 | 96.6% |
Reaction Steps
Trifluoroacetic acid (TFA, 0.5 ml) and dichloromethane (0.5 ml) was added to 20 mg of 5. The mixture was shaken at room temperature for 1 h and the volatile materials was then removed at reduced pressure to give 18 mg of 6 as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040637B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-eb95f250a61747419efdaa224febe94d |
| Source note | uspto-grants-2015_05 |