HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicyl Alcohol → HCID 58022302, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicyl Alcohol | HCID 5146 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | (2-Bromoethoxy)-tert-butyldimethylsilane | HCID 3608067 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 58022302 | HCID 58022302 | — |
Reaction Steps
To a suspension of 2-hydroxybenzyl alcohol (0.4 g) and potassium carbonate (0.67 g) in N,N-dimethylformamide (6 mL) was added 2-(tert-butyldimethylsilyloxy)ethyl bromide (1.05 mL), and the mixture was stirred at room temperature overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040693B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-211d0be47772441ca70d712dfe696ebf |
| Source note | uspto-grants-2015_05 |