HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxy-N-methylpropan-1-amine → HCID 178495288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxy-N-methylpropan-1-amine | HCID 12545984 | — |
| Reactant | HCID 178492256 | HCID 178492256 | — |
| Product | HCID 178495288 | HCID 178495288 | — |
Reaction Steps
The title compound was prepared in a manner similar to Example 227 using 6-(4-(4-cyano-2-methoxyphenyl)-5-hydroxy-1H-pyrazol-1-yl)nicotinic acid and 3-methoxy-N-methylpropan-1-amine 1H NMR (400 MHz, DMSO-d6) δ ppm 1.76-2.04 (m, 2 H) 3.09 (d, J=7.3 Hz, 3 H) 3.21 (s, 2 H) 3.36 (s, 2 H) 3.43-3.56 (m, 2 H) 3.65 (t, J=6.9 Hz, 1 H) 3.98 (s, 3 H) 7.31-7.36 (m, 2 H) 8.05 (br. s., 1 H) 8.28-8.64 (m, 3 H). MS m/z [M+H]+ 422.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040522B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-05d8722b17424e36834115ce5ae38990 |
| Source note | uspto-grants-2015_05 |