HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 4-(2,6-Diethyl-4-methylphenyl)-2,6-dimethyl-5-methylsulfonyl-2,3-dihydro-3-pyridazinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-[2-(2,6-Diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-(1-methylsulfonyl-2-propylidene)hydrazine | HCID 76468960 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-(2,6-Diethyl-4-methylphenyl)-2,6-dimethyl-5-methylsulfonyl-2,3-dihydro-3-pyridazinone | HCID 56942717 | — |
Reaction Steps
To a test tube (outside diameter: 21 mm Φ×overall length: 160 mm), 1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-(1-methylsulfonyl-2-propylidene)hydrazine ((4-34-(1)-39) (201.0 mg), potassium carbonate (115.1 mg), and methanol (757 μl) were added under ice-cooling.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040709B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-f4672f69d9bc4df78a4a538b501bb81c |
| Source note | uspto-grants-2015_05 |