huagongshe.com
HRID5794

反应详情

EQUATION

反应方程式

HRID 5794 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)N1CCNCC1
HCID83795

1-Acetylpiperazine

C6H12N2O

结构：CC1CCN(c2cc3nc(C(C)(C)C)sc3cc2N=C=S)CC1
HCID15610362

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)N1CCN(C(=S)Nc2cc3sc(C(C)(C)C)nc3cc2N2CCC(C)CC2)CC1
HCID54175931

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

A solution of 2.0 g of 2-tert-butyl-6-isothiocyanato-5-(4-methylpiperidin-1-yl)benzothiazole and 0.78 g of 1-acetyl-piperazine in 30 ml of chloroform is stirred for 30 minutes and the product triturated with petroleum ether to obtain 6-[(4-acetyl-piperazin-1-yl)thiocarbonylamino]-2-tert-butyl-5-(4-methylpiperidin-1-yl)benzothiazole, melting at 187°-190°.

WORKUP

后处理

  1. customthe product triturated with petroleum ether