HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 86683403, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 86683402 | HCID 86683402 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86683403 | HCID 86683403 | 100% |
Reaction Steps
A mixture of 2-(imidazole-1-carbonyl)-6-methoxy-1,2,3,4-tetrahydro-isoquinoline-5-carbaldehyde (426 mg, 1.50 mmol) and methyl iodide (475 μL, 1.05 g, 7.6 mmol) in anhydrous acetonitrile (10 mL) was stirred at room temperature for 24 h. After evaporation of the solvent the title compound (640 mg, 1.50 mmol, 100%) was obtained as a brownish foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040714B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-fad8432ff4754b618bcfd1be862b9f23 |
| Source note | uspto-grants-2015_05 |