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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 579429Generated: October 31, 2026

Methyl iodide → HCID 86683403, compound

https://huagongshe.com/reaction/579429

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantHCID 86683402HCID 86683402—
SolventAcetonitrileHCID 6342—
ProductHCID 86683403HCID 86683403100%

Reaction Steps

A mixture of 2-(imidazole-1-carbonyl)-6-methoxy-1,2,3,4-tetrahydro-isoquinoline-5-carbaldehyde (426 mg, 1.50 mmol) and methyl iodide (475 μL, 1.05 g, 7.6 mmol) in anhydrous acetonitrile (10 mL) was stirred at room temperature for 24 h. After evaporation of the solvent the title compound (640 mg, 1.50 mmol, 100%) was obtained as a brownish foam.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09040714B2
Source datasetuspto-grants-2015_05
ORD IDord-fad8432ff4754b618bcfd1be862b9f23
Source noteuspto-grants-2015_05