HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 57668844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 6620889 | HCID 6620889 | — |
| Product | HCID 57668844 | HCID 57668844 | 84% |
Reaction Steps
The procedure for the synthesis of 2 was followed (1 eq. NBS was used) to prepare 3 from 1 as white crystals in an 84% yield. 1H NMR (400 MHz, CDCl3, 298 K): δ(ppm) 8.20-8.19 (d, 1H), 8.05-8.03 (d, 1H), 7.53-7.38 (m, 3H), 7.28-7.21 (m, 2H), 4.04-4.02 (d, 2H), 2.32-2.30 (m, 1H), 0.97-0.94 (d, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040718B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-04b22a9ca0b24473b956b1f5b624d24b |
| Source note | uspto-grants-2015_05 |