Hydrochloric Acid → HCID 70400181, compound

Participants

Reaction Steps

52.1 g of 35% hydrochloric acid and 13.4 g of water were added to 69.6 g (0.5 mole) of N-cyclohexylallylamine under cooling to obtain a 65.0% aqueous solution of N-cyclohexylallylamine hydrochloride. This solution was added with 1.054 g (0.600 mol % based on the monomer) of initiator (1) and polymerized at 60° C. for 48 hours. The resulting reaction product was treated in the same way as in Example 1 to obtain 61.8 g of white powder (rate of polymerization: 70.3%). In the IR absorption spectrum of this product, absorption at 930 cm-1 and 990 cm-1 disappeared. Intrinsic viscosity (ηinh) of this polymer was 0.72.

Provenance & Evidence