Water → HCID 86742221, compound

HRID 579999Notes

Reaction equation

HRID 579999 reaction equation
[Cl:1][C:2]1[C:14]([Cl:15])=[C:13](/[CH:16]=[C:17](/[N+:20]([O-:22])=[O:21])\[CH2:18][CH3:19])[CH:12]=[CH:11][C:3]=1[O:4][CH2:5][CH2:6][CH2:7][C:8]([OH:10])=[O:9].O.C(=O)(O)[O-].[Na+:28]>>[Cl:1][C:2]1[C:14]([Cl:15])=[C:13](/[CH:16]=[C:17](/[N+:20]([O-:22])=[O:21])\[CH2:18][CH3:19])[CH:12]=[CH:11][C:3]=1[O:4][CH2:5][CH2:6][CH2:7][C:8]([O-:10])=[O:9].[Na+:28]

Participants

4

Reactant 3

HCID 962WaterHCID 516892Sodium BicarbonateHCID 12290540HCID 12290540, compound

Product 1

HCID 86742221HCID 86742221, compound

Procedure

250 mg of (E)-4-[2,3-dichloro-4-(2-nitro-1-butenyl)phenoxy]butyric acid is dissolved in 3.1 ml of 0.1 N sodium bicarbonate and sufficient isotonic buffer to make a final volume of 10 ml. The water from all sources was pyrogen-free. The solution is sterilized by filtration.

Workup

  1. filtrationThe solution is sterilized by filtration

Sources & evidence

ORD record
ord-fd8dd96b6a1a474dafc33884a6342434
Source dataset
uspto-grants-1988_06
Patent number
US04751244

Reaction notes

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