Water → HCID 86742222, compound

HRID 580000Notes

Reaction equation

HRID 580000 reaction equation
[Cl:1][C:2]1[C:15]([Cl:16])=[C:14](/[CH:17]=[C:18](/[N+:21]([O-:23])=[O:22])\[CH2:19][CH3:20])[CH:13]=[CH:12][C:3]=1[O:4][C:5]1([C:9]([OH:11])=[O:10])[CH2:8][CH2:7][CH2:6]1.O.C(=O)(O)[O-].[Na+:29]>>[Cl:1][C:2]1[C:15]([Cl:16])=[C:14](/[CH:17]=[C:18](/[N+:21]([O-:23])=[O:22])\[CH2:19][CH3:20])[CH:13]=[CH:12][C:3]=1[O:4][C:5]1([C:9]([O-:11])=[O:10])[CH2:8][CH2:7][CH2:6]1.[Na+:29]

Participants

4

Reactant 3

HCID 962WaterHCID 516892Sodium BicarbonateHCID 20135562HCID 20135562, compound

Product 1

HCID 86742222HCID 86742222, compound

Procedure

250 mg of (E)-1-[2,3-dichloro-4-(2-nitro-1-butenyl)phenoxy]cyclobutane-1-carboxylic acid is dissolved in 31 ml of 0.1 N sodium bicarbonate and sufficient isotonic buffer to make a final volume of 100 ml. The water from all sources was pyrogen-free. The solution is sterilized by filtration.

Workup

  1. filtrationThe solution is sterilized by filtration

Sources & evidence

ORD record
ord-3d4384e6247d4481a1868f3913bc6e85
Source dataset
uspto-grants-1988_06
Patent number
US04751244

Reaction notes

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