HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1-(3-Diethylaminopropyl)-3-(3-diethylaminopropylamino)-5-aminoindazole trihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 1-(3-Diethylaminopropyl)-3-(3-diethylaminopropylamino)-5-aminoindazole | HCID 20135837 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(3-Diethylaminopropyl)-3-(3-diethylaminopropylamino)-5-aminoindazole trihydrochloride | HCID 20135879 | — |
Reaction Steps
In 15 ml of absolute ethyl alcohol was dissolved 0.7 g of the 1-(3-diethylaminopropyl)-3-(3-diethylaminopropylamino)-5 -aminoindazole, and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Then to the solution was added anhydrous diethyl ether to separate crystals. The crystals were obtained by filtration and dried to give 1-(3-diethylaminopropyl)-3-(3-diethylaminopropylamino)-5-aminoindazole trihydrochloride having the following analytical value.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04751302 |
| Source dataset | uspto-grants-1988_06 |
| ORD ID | ord-933d3d0c3b2447ef8b3a15d27e08d147 |
| Source note | uspto-grants-1988_06 |