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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 58025Generated: October 30, 2026

HCID 89800236, compound → HCID 89800333, compound

https://huagongshe.com/reaction/58025

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 89800236HCID 89800236—
ReactantHCID 178418361HCID 178418361—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductHCID 89800333HCID 89800333—

Reaction Steps

N-phenylacetyl-D,L-leucyl-L-proline benzyl ester (2 g) was dissolved in methanol (40 ml), and 10% palladium-carbon (200 mg) was added. The resulting mixture aerated with hydrogen was allowed to react at room temperature for 3 h, filtered and concentrated under reduced pressure to remove the solvent to give a colourless sticky matter (1.55 g, 98%), which was directly used for the next reaction.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09434760B2
Source datasetuspto-grants-2016_09
ORD IDord-dc6887c10f434b009b85da277eb38fe3
Source noteuspto-grants-2016_09