HCID 14229389, compound → HCID 14229390, compound

HRID 580505Notes

Reaction equation

HRID 580505 reaction equation
[NH2:1][C:2]1[C:11]2[CH:10]=[CH:9][N:8]=[CH:7][C:6]=2[N:5]=[C:4]2[CH2:12][CH2:13][CH2:14][C:15](=[O:16])[C:3]=12.[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[NH2:1][C:2]1[C:11]2[CH:10]=[CH:9][N:8]=[CH:7][C:6]=2[N:5]=[C:4]2[CH2:12][CH2:13][CH2:14][CH:15]([OH:16])[C:3]=12

Participants

4

Reactant 2

HCID 14229389HCID 14229389, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 14229390HCID 14229390, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

To a cooled solution of 5-amino-6,7,8,9-tetrahydrobenzo[b][1,7]naphthyridin-6-one (3.05 g) was added 14.5 ml of 1M lithium aluminum hydride in tetrahydrofuran. This was stirred for 1 hour.

Sources & evidence

ORD record
ord-83905a109f3342eeb4773f80d233258c
Source dataset
uspto-grants-1988_06
Patent number
US04753950

Reaction notes

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