HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54365084, compound → HCID 86742243, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54365084 | HCID 54365084 | — |
| Reactant | HCID 86742244 | HCID 86742244 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 86742243 | HCID 86742243 | — |
Reaction Steps
2.97 g (10 mmol) of 1-(-2-benzyloxyphenyl)-2-nitro-1-buten-3-one and 2.96 g (mmol) of 3-aminocrotonic acid 4-(2-trifluoromethylphenylethyl)piperazide are heated in 15 ml of isopropanol at 60° C. for 4 hours. After cooling, a crude product is obtained, and this is recrystallized from a littel ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04753936 |
| Source dataset | uspto-grants-1988_06 |
| ORD ID | ord-452d18c95e5c48fa949bbd6afed65a68 |
| Source note | uspto-grants-1988_06 |