HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Nitroprop-1-en-2-amine → HCID 86742245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Nitroprop-1-en-2-amine | HCID 71404712 | — |
| Reactant | HCID 86162491 | HCID 86162491 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 86742245 | HCID 86742245 | — |
Reaction Steps
2.5 g (10 mmol) of crude 2-acetyl-3-(3-nitrophenyl)-2-propenoic acid 4-phenyl-piperazide and 2.5 g (25 mmol) of 2-amino-1-nitro-1-propene are heated in 15 ml of isopropanol at 60° C. for 6 hours. The crude product which has precipitated out is crystallized from isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04753936 |
| Source dataset | uspto-grants-1988_06 |
| ORD ID | ord-f503b39e6e1d4a8fb286936bffd064ce |
| Source note | uspto-grants-1988_06 |