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HRID580515

反应详情

EQUATION

反应方程式

HRID 580515 的结构方程式

REACTANTS

反应物

2
结构：CC(N)=C[N+](=O)[O-]
HCID71404712

1-Nitroprop-1-en-2-amine

C3H6N2O2

结构：CC(=O)C(=Cc1cccc([N+](=O)[O-])c1)C(=O)N1CCN(c2ccccc2)CC1
HCID86162491

未命名化合物

PRODUCTS

生成物

1
结构：CC1=C(C(=O)N2CCN(c3ccccc3)CC2)C(c2cccc([N+](=O)[O-])c2)C([N+](=O)[O-])=C(C)N1
HCID86742245

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)O
溶剂HCID3776

Isopropanol

C3H8O

PROCEDURE

实验过程

2.5 g (10 mmol) of crude 2-acetyl-3-(3-nitrophenyl)-2-propenoic acid 4-phenyl-piperazide and 2.5 g (25 mmol) of 2-amino-1-nitro-1-propene are heated in 15 ml of isopropanol at 60° C. for 6 hours. The crude product which has precipitated out is crystallized from isopropanol.

WORKUP

后处理

  1. customThe crude product which has precipitated out
  2. customis crystallized from isopropanol