Hydrochloric Acid → HCID 178423001, compound

HRID 580520Notes

Reaction equation

HRID 580520 reaction equation
[CH3:1][C:2]1[CH:6]=[C:5]([C:7]2[NH:8][C:9]3[C:18]4[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=4[N:12]=[CH:11][C:10]=3[N:19]=2)[O:4][N:3]=1.[ClH:20]>>[ClH:20].[CH3:1][C:2]1[CH:6]=[C:5]([C:7]2[NH:8][C:9]3[C:18]4[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=4[N:12]=[CH:11][C:10]=3[N:19]=2)[O:4][N:3]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 178423000HCID 178423000, compound

Product 1

HCID 178423001HCID 178423001, compound

Procedure

To an ethanolic solution of 300 mg of 2-(3-methylisoxazol-5-yl)-1H-imidazo[4,5-c]quinoline C45 is added ethanolic hydrogen chloride at room temperature. The mixture is evaporated and the residue is washed with acetone to give C100 as crystals melting at 248.5°-252° C. (dec.).

Workup

  1. customThe mixture is evaporated
  2. washthe residue is washed with acetone

Sources & evidence

ORD record
ord-676736dbb0b744de96e4f686abab48d3
Source dataset
uspto-grants-1988_06
Patent number
US04753951

Reaction notes

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