反应详情

温度

70 °C

To a 4 mL vial equipped with a magnetic stir bar were added 5-bromopyridine-2-sulfonyl chloride hydrochloride (250 mg, 0.853 mmol) and ammonium hydroxide (1329 μL, 34.1 mmol) to give a white suspension, which was heated to 70° C. in a sand bath overnight. The solvent was subsequently evaporated to give the title compound, which was used without further purification.

1. customTo a 4 mL vial equipped with a magnetic stir bar
2. customto give a white suspension, which
3. customThe solvent was subsequently evaporated