HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 20133950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 20133960 | HCID 20133960 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20133950 | HCID 20133950 | — |
Reaction Steps
The equimolar amount of sodium methylate is added at room temperature to 1.0 g (0.0025 mole) of 1,3-dimethyl-5-[4-(6-chloropyridazin-3-yloxy)phenylcarbamoyl]barbituric acid in 20 ml of methanol. The mixture is heated under reflux for 5 hours, then cooled, diluted with water and filtered. The filtrate is washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04753940 |
| Source dataset | uspto-grants-1988_06 |
| ORD ID | ord-fa57ca4cc81d4453b454e3d3f4070a94 |
| Source note | uspto-grants-1988_06 |