HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dimethyl-5-ethoxycarbonylbarbituric acid → HCID 20133968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dimethyl-5-ethoxycarbonylbarbituric acid | HCID 593714 | — |
| Reactant | 4-(Quinolin-2-yloxy)aniline | HCID 13108946 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20133968 | HCID 20133968 | — |
Reaction Steps
6.1 g of 4-(quinolin-2-yloxy)aniline and 5.8 g of 1,3-dimethyl-5-ethoxycarbonylbarbituric acid are heated under reflux in 50 ml of toluene. When the temperature is at 80° C., a thick crystalline slurry is formed which at 120° C. is again of a stirrable consistency. After stirring for 3 hours, the mixture is cooled and the crystals are isolated by suction filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04753940 |
| Source dataset | uspto-grants-1988_06 |
| ORD ID | ord-5f781abe18c04b42b6b239bd41b0c6b4 |
| Source note | uspto-grants-1988_06 |